Rose oil Gas chromatography mass spectrometry (GCMS) testing

Bulgarian Rose Oil a/k/a Rose otto, or Attar of Roses RoseOil. Produced in Bulgaria by the Bulgarian OrganiRose Co the Standard bearer of the Rose oil!


Identification information of the Rose oil under investigation:

BPG Ref. No: EB000111303_002_16 rose oil gc/ms testing

I# 119634-4467; Batch 1/2000, Cont. No 590 06.10.2000, A/c 576 09.10.2000

The data presented below is accurate and complete representation of an actual testing certificate from testing performed by M/S Nishant Aromas of New Delhi, India. The testing was requested and is a generous contribution of Mr. Christopher McMahon of White Lotus Aromatics of El Cerrito, California 94530.

Company Name: M/S Nishant Aromas

Sample Name: c:\anatec\ROSE\ROSE OIL OTTO BULGARIA FFAP 50.dat

Date: 23rd Apr. 2001 Time: 15:13:04

Method Name: Default.Mtd

PW SLP PWDT AREJ HREJ BSSTV SKM
10 25 99.99 50 14 8 .1
RAW DATA NORMAL ISATION REPORT - Normal Page 1
PEAK NO P.TIME (Min) PEAK HT (mV) AREA (mv-sec)

AMOUNT AREA %

TYPE PEAK NAME
1 3.55 282 1,034 0.940 BB
2 4.78 149 661 0.601 VB A-Pinene 1039
3 6.52 25 170 0.154 BB
4 7.85 74 507 0.461 BV Myrceen 1156
5 8.48 18 203 0.184 VV Heptanol 1186
6 8.72 16 175 0.159 VB Limonene 1206
7 12.60 77 610 0.555 BV Cis Rose Oxide 1354
8 12.97 31 255 0.232 VB Trans Rose Oxide 1370
9 15.68 17 222 0.202 BV
10 15.98 30 561 0.510 VV Decanal 1485
11 17.10 523 2,363 2.148 VB Linalool 1505
12 18.15 75 613 0.557 BV Terpine-4-ol 1597
13 18.37 117 893 0.812 VB B-Caryophyllene 1617+Citronellyl Act 1645
14 19.63 93 628 0.570 BV Iso Borneol 1660
15 19.95 49 436 0.396 VV Neral 1661
16 20.23 103 591 0.537 VV Benzyl Acetate 1697
17 20.47 252 1,557 1.415 VV Neryal Acetate 1699
18 20.56 292 1,516 1.378 VV Citronellyl Propionate 1700
19 20.82 106 1,484 1.349 VV Geranial 1706
20 21.30 186 1,012 0.920 VV Heptadecane
21 21.48 15 229 0.208 VV
22 21.63 126 838 0.762 VV
23 22.02 3,068 33,351 30.314 VV Citronellol 822
24 22.32 31 301 0.274 VV Geranyl Acetate 1735
25 22.65 1,540 9,306 8.458 VV Nerol 1757
26 22.78 66 520 0.473 VV Phenyl Ethyl Acetate 1785
27 23.07 54 429 0.390 VV Geranyl Iso Butyrate 1795
28 23.60 2,343 18,665 16.965 VB Geraniol 1797
29 24.72 995 13,862 12.599 BV Phenyl Ethyl Alcohol 1859
30 24.87 400 3,000 2.726 VV Nonadecane 1900
31 24.97 588 2,746 2.496 VB
32 26.38 168 1,104 1.004 BV B-Ionone 1918
33 26.67 21 211 0.191 VV Cis-Nerolidol 1961
34 26.87 326 1,815 1.650 VV Ecosane 2000
35 27.15 25 175 0.159 VB Methyl Eugenol 2023
36 28.57 366 4,067 3.696 BV Hexacosane 2100
37 28.77 16 97 0.088 VB Eugenol 2103
38 29.20 15 99 0.090 BB
39 30.43 185 1,399 1.272 BV Docacosane 2200
40 30.72 16 153 0.139 VB
41 32.07 14 103 0.094 BB
42 33.77 57 369 0.335 BB Tricosane 2300
43 34.47 23 192 0.175 BB
44 36.07 165 1,498 1.361 BB Farnesol 2350
Total 13,138 110,021

CHROMWIN ' Developed by Anatec Instruments - New Delhi: Tel: 5438193, 5158459

Approved By: STARTED AT 60 DEG. HOLD 2 MIN. RATE 6 C/MIN. PRESSURE 6 PSIG SAMPLE SIZE 0.03ML

Remarks:

Carrier: Nitrogen @ 30 ml/min Fuel: Hydrogen @ 30ml/min. Oxidant: Zero Air @ 300 ml/min

Column: 300mm x 0.25 mm FFAP POLAR CAPILLARY COLUMN Detector: F.I.D.

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